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水泥技术, 2026, 1(3): 63-67    doi: 10.19698/j.cnki.1001-6171.20263063
  材料研究 本期目录 | 过刊浏览 | 高级检索 |
碱石棉吸收称量法测定水泥中石灰石含量的影响因素研究
冯蕾
山东省产品质量检验研究院,山东  济南  250022
Investigation on the Influencing Factors of the Content of Limestone in Cement by Alkali Asbestos Absorption Weighing Method
FENG Lei
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摘要 为探究采用碱石棉吸收称量法测定水泥中石灰石含量结果不稳定的原因,本文通过实验测试了石灰石品位、吸收装置U型管称量方式、碱石棉吸收剂品质、反应液微沸时间及通气速率等因素对测定结果的影响。实验表明,石灰石品位越低,测定结果负偏差越大;采用将吸收装置U型管竖直放置于烧杯中的称量方式,其稳定性优于直接水平放置;碱石棉吸收剂性能差异直接影响测定结果的准确性;反应液微沸时间<4min会导致检测结果严重偏低;通气速率存在最佳范围(3~5气泡/秒),速率过快或过慢均会因CO2气体吸收不完全或系统压力变化而导致测定结果出现误差。最后提出结论,严格控制实验样品品质、规范操作步骤并运用性能稳定的碱石棉吸收剂,是提升测定结果准确性的关键。
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冯蕾
关键词:  石灰石含量  碳酸钙  碱石棉吸收称量法  吸收剂  影响因素    
Abstract: To explore the reasons for the unstable results of the determination of limestone content in cement by the alkali asbestos absorption weighting method, this paper experimentally tested the effects of factors such as limestone grade, weighing method of the U-tube in the absorption device, quality of the alkali asbestos absorbent, micro-boiling time of the reaction solution, and gas flow rate on the determination results. The experiments showed that the lower the limestone grade, the greater the negative deviation of the determination results; the stability of the weighing method where the U-tube of the absorption device is placed vertically in the beaker is better than that of the direct horizontal placement; the performance difference of the alkali asbestos absorbent directly affects the accuracy of the determination results; a micro-boiling time of the reaction solution < 4min would lead to a significant underestimation of the detection results; there is an optimal range for the gas flow rate (3~5 bubbles per second), and rates that are too fast or too slow would introduce errors in the determination results due to incomplete absorption of CO2 gas or changes in system pressure. Finally, it is proposed that strictly controlling the quality of the experimental samples, standardizing the operation steps, and using alkali asbestos absorbents with stable performance are the keys to improving the accuracy of the determination results.
Key words:  limestone content    calcium carbonate    alkali asbestos absorption weighting method    absorbent    influencing factors
收稿日期:  2025-09-04                出版日期:  2026-05-25      发布日期:  2026-05-25      整期出版日期:  2026-05-25
ZTFLH:  TQ172.1  
作者简介:  冯蕾(1989—),女,助理工程师,主要从事水泥等建材质量检验研究。E-mail:616949881@qq.com
引用本文:    
冯蕾. 碱石棉吸收称量法测定水泥中石灰石含量的影响因素研究[J]. 水泥技术, 2026, 1(3): 63-67.
FENG Lei. Investigation on the Influencing Factors of the Content of Limestone in Cement by Alkali Asbestos Absorption Weighing Method. Cement Technology, 2026, 1(3): 63-67.
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http://www.cemteck.com/CN/10.19698/j.cnki.1001-6171.20263063  或          http://www.cemteck.com/CN/Y2026/V1/I3/63
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